Semiconductors & Microelectronics

Broad-area screening to targeted elemental insight — from wafers and dies to packages, boards, and trace samples.

Atlas microXRF non-destructively maps wafers, dies, packages, boards, and trace samples, distinguishing process materials and contaminants through spatially resolved elemental analysis. It combines large-area surveys with targeted sub-maps and line scans in one workflow, supporting failure analysis, process monitoring, contamination control, and incoming inspection.

With ultra-high spatial resolution and broad elemental coverage (C to U), Atlas is suited for verifying gallium nitride wafers, silicon carbide, and other compound semiconductor materials — connecting wafer-scale screening with targeted follow-up so teams can locate issues quickly without destroying valuable samples.

Close-up of a semiconductor chip package with gold pins, alongside five microXRF elemental maps of the same package
The Workflow

Elemental Insight From Assembly to Defect

Three stages of the same workflow, on one platform — no switching instruments between them.

1

Screen Complete Assemblies

Map material composition and elemental variation across boards, components, traces, and complex assemblies.

2

Localize Microscopic Defects

Find contamination, residues, or anomalous features, then target them with high-resolution sub-maps.

3

Verify Materials & Processes

Evaluate metallization, coatings, layer behavior, and process variation non-destructively.

High-Resolution Analysis of Interconnects and Contamination

5 µm mapping resolving individual wire bonds and packaging residues on a real quad flat package.

MicroXRF elemental map of gold wire bonds and the silver lead frame of a quad flat package, overlaid on an optical image

Real Contamination Map

K/Ca overlay on the same package — scattered particle-like residues visible against the substrate, exactly the kind of localized packaging contamination a bulk measurement can't isolate.

IXRF applications scientist holding a QFP chip, with an inset K/Ca map showing scattered contamination particles

QFP Package Under Test

The real quad flat package these maps were collected from — for reference alongside the elemental overlays above.

Quad flat package shown half as an optical image and half as an Ag, Au and Cu elemental map
Real Quantification Data

5 µm Sub-Mapping Resolves Contamination Missed by Bulk Measurements

Three real, quantified solder-related contamination sites from an actual sub-map overlay. Three localized features show measurable Sn and Pb together with Au, consistent with solder-related contamination or residue — invisible to a bulk-composition measurement.

Concentration (wt%)
LocationFeNiCuSnAuPb
10.0574.4020.920.244.310.91
20.0367.1020.898.001.862.12
30.0565.1421.274.386.622.54
MicroXRF sub-map overlay showing three solder-related contamination sites labelled 1 to 3Optical image of the same area with the three measured locations marked
Three localized features show measurable Sn and Pb together with Au, consistent with solder-related contamination or residue.

Composition Comparison Across Many Locations

Ten real bump measurements from one wafer, with automatically calculated statistics. Map-based quantification compares bump composition across many locations on the same sample — a full X-ray spectrum is captured at each point, and ‘Go To’ stage navigation returns users to specific features for follow-up work.

Bump composition (wt%)
SampleAg (wt%)Sn (wt%)
Center-11.498.6
Center-21.398.7
Center-31.598.5
Center-41.398.7
Center-52.098.0
Center-61.698.5
Center-71.398.8
Center-81.598.5
Center-91.398.7
Center-101.698.4
Mean1.598.5
Std. Dev.0.20.2
Min / Max1.3 / 2.098.0 / 98.7
Grid of microXRF maps of solder bump arrays on a wafer, with the ten measured bump locations numbered

Multi-Layer Thin Film Analysis

Non-Destructive Thickness and Composition Measurement

Up to 8 layers plus infinite substrate, modeled without cross-sectioning the part.

  • Measures large components while targeting microscopic regions with up to 5 µm spatial resolution
  • Supports up to 8 layers plus infinite substrate using Fundamental Parameters modeling
  • Reveals thickness variation across plated parts
MicroXRF capillary measuring plating thickness on gold-plated PCB contacts, with an inset elemental map of the board

Wafer & Die Mapping

Screen Uniformity, Reveal Elemental Variation

Wafer-scale surveys followed immediately by targeted sub-maps, in one workflow.

Wafer-scale maps quickly highlight non-uniformity, missing or altered dies, and spatial trends. Elemental overlays separate Si, Cu, Ta, Ni, and other process materials across patterned structures. Thermal-scale maps reveal gradients that may not be obvious in optical images alone — large-area maps can be followed immediately by sub-maps on selected regions of interest.

Once an elemental map is generated, users can define regions of interest to create higher-resolution sub-maps for targeted analysis — isolating localized contamination, trace residues, and subtle element differences. A sub-region of a sub-map can be re-mapped when even more detail is needed.

Diced wafer in a carrier dish, with circular microXRF maps of Si, Ti, Ni and Hf distribution
Applications

Circuit Boards, Lead Frames, and Wafer Metrology

Four established real use cases, each with its own specific analytical questions.

Circuit Board Inspection

  • Fast X-ray mapping for electronics inspections
  • A complete X-ray spectrum for each pixel in the map
  • Measure thin gold and palladium coatings on PCBs
  • Measure coating thickness of Cu, Ni, etc.
  • Measure solder composition
  • RoHS / WEEE compliance

Lead Frame Imaging

  • Measurements on very small flat components — conducting paths, contacts, lead frames
  • Multi-coating systems (e.g., AuAg/Pd/Ni/CuFe) in the nanometer range
  • Determination of phosphorus content in NiP coatings
  • Functional coatings in electronics and semiconductor industries

Wafer Metrology

  • Sn/Ag bump and pillar measurements
  • Light-element detection
  • Metal film stack composition, such as CIGS
  • Cu CMP control at BEOL

Wafer Metrology (continued)

  • Multi-stack structures
  • Sputtering targets
  • Thermal barrier coating
  • Thickness and composition control
Which Method Fits

MicroXRF Compared With Other Semiconductor-Analysis Methods

MicroXRF's advantage is coverage and non-destructive workflow, not finer resolution than SEM.

vs. SEM-EDS

SEM-EDS resolves finer features and combines elemental data with detailed imaging, but typically requires a smaller, prepared, conductive-coated sample inside the chamber. MicroXRF covers full boards, wafers, and packages non-destructively — often used to screen broadly before a targeted SEM-EDS follow-up on a flagged region.

vs. Cross-Sectioning

Physical cross-sectioning destroys the part to reveal layer structure. MicroXRF's Fundamental Parameters modeling quantifies multilayer thickness and composition non-destructively — the part can still be used, shipped, or re-measured after analysis.

Get in touch with our experts

See What MicroXRF Can Find in Your Assembly

Describe your board, wafer, package, or component type and the elemental question you're trying to answer. An IXRF applications scientist can help determine whether microXRF is the right fit and discuss sample feasibility before instrument selection.

Atlas Apex microXRF spectrometer with its sample chamber open
FAQ

Frequently
Asked Questions

Atlas Apex can analyze wafers, wafer sections, substrates, and other planar microelectronic samples. Atlas Apex M provides automated mapping over areas up to approximately 220 × 200 mm, while Atlas Apex X provides greater flexibility for larger wafers, assemblies, and samples that exceed the chamber-based system’s practical dimensions.

Yes. MicroXRF can non-destructively measure the composition and thickness of multilayer coatings and thin films when the layer materials and structure are suitable for XRF analysis. Iridium Ultra supports thin-film Fundamental Parameters analysis for structures containing up to eight layers plus a substrate.

Yes. Atlas Apex can create high-resolution elemental maps of interconnects, wire bonds, solder features, metallization, contacts, and other microelectronic structures. Focused X-ray spot sizes down to approximately 5 µm are available, although actual spatial resolution depends on the elements, materials, and sample geometry being analyzed.

Yes. MicroXRF can map elemental distributions across wafers, coatings, and deposited films to identify composition gradients, non-uniform deposition, localized enrichment, contamination, and process-related variation. Each Atlas Apex mapping pixel retains a complete X-ray spectrum for subsequent analysis.

Yes. Atlas Apex can automate measurements across multiple solder bumps, pads, contacts, or other predefined locations and compare their elemental composition. Automated positioning and mapping make it possible to identify lot-to-lot, device-to-device, or location-to-location compositional variation efficiently.

Yes. MicroXRF is highly effective for locating and identifying many forms of metallic contamination, foreign material, plating anomalies, elemental inclusions, and compositional defects. Elemental mapping can show both the chemistry and spatial distribution of anomalous material without requiring destructive sectioning in many applications.

Yes. Because X-rays penetrate more deeply than the electron beam used in SEM-EDS, Atlas Apex can often analyze packaged components, circuit boards, connectors, solder joints, and electronic assemblies without cross-sectioning. The accessible depth depends on the materials, layer thicknesses, elements of interest, and device geometry.

Yes. MicroXRF can rapidly screen electronic materials for elements associated with RoHS restrictions, including lead, mercury, cadmium, chromium, and bromine. XRF measures elemental composition, however, so additional analytical techniques may be required when regulations depend on chemical form or molecular species, such as hexavalent chromium or specific brominated flame retardants.

MicroXRF and SEM-EDS provide complementary information. SEM-EDS offers much higher spatial resolution for very small features, while MicroXRF provides larger-area mapping, greater X-ray penetration, strong trace-element sensitivity, and analysis of larger samples with minimal preparation. MicroXRF can therefore locate compositional anomalies over a broad area before SEM-EDS is used for detailed investigation.

Atlas Apex can analyze a wide range of semiconductor and electronic materials, including silicon wafers, metallization layers, solder alloys, wire bonds, contacts, interconnects, lead frames, coatings, ceramic substrates, printed circuit boards, electronic components, and packaged devices. Applications range from R&D and process development to quality control and failure analysis.